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含イオウシアナミド誘導体の熱分解生成物のIR,UVおよびX線回折による検討
https://doi.org/10.15099/00004069
https://doi.org/10.15099/0000406935e8e666-7aaa-46e5-ba74-1fc827beb638
名前 / ファイル | ライセンス | アクション |
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Kokiyo_22_01_Page027to032.pdf (1.9 MB)
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Item type | 紀要論文 / Departmental Bulletin Paper(1) | |||||
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公開日 | 2012-08-20 | |||||
タイトル | ||||||
タイトル | 含イオウシアナミド誘導体の熱分解生成物のIR,UVおよびX線回折による検討 | |||||
言語 | ||||||
言語 | jpn | |||||
キーワード | ||||||
主題Scheme | Other | |||||
主題 | 含イオウシアナミド誘導体 | |||||
キーワード | ||||||
主題Scheme | Other | |||||
主題 | 熱分解生成物 | |||||
キーワード | ||||||
主題Scheme | Other | |||||
主題 | X線回析 | |||||
キーワード | ||||||
主題Scheme | Other | |||||
主題 | 赤外吸収スペクトル | |||||
キーワード | ||||||
主題Scheme | Other | |||||
主題 | 紫外吸収スペクトル | |||||
キーワード | ||||||
主題Scheme | Other | |||||
主題 | 熱分解機構 | |||||
資源タイプ | ||||||
資源タイプ識別子 | http://purl.org/coar/resource_type/c_6501 | |||||
資源タイプ | departmental bulletin paper | |||||
ID登録 | ||||||
ID登録 | 10.15099/00004069 | |||||
ID登録タイプ | JaLC | |||||
著者 |
浅岡, 忠知
× 浅岡, 忠知× 島崎, 長一郎× 堀, 修平 |
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著者別名 | ||||||
姓名 | ASAOKA, Tadatomo | |||||
著者別名 | ||||||
姓名 | SHIMASAKI, Chouichiro | |||||
著者別名 | ||||||
姓名 | HORI, Shuhei | |||||
その他(別言語等)のタイトル | ||||||
その他のタイトル | Studies on Thermal-Decomposition of Sulfur containing Noncyclic Cyanamide Derivatives by IR, UV and X-ray Techniques | |||||
抄録 | ||||||
内容記述タイプ | Abstract | |||||
内容記述 | Using thiourea, ammonium thiocyanate, 2.4-dithiobiuret and guanylthiourea belonging to sulfur containing noncyclic cyanamide derivatives, these decomposition compounds was follwed by utilizing the IR, UV and X-ray diffraction techniques. From IR remarking the bending band of triazine ring corresponded to 800cm^<-1>, the temperatures at which respective compounds cyclize are determined. In UV, the absorption of ammeline, ammelide, melam, melem, thioammeline are clearly decided from which could also be followed the proceeding of cyclization. And, in X-ray diffraction the changes of intermedates in the thermal decomposition are checked as it were qualitative owing to the important information that the diffraction line becomes simple as the cyclization increases. Combining these three techniques mentioned above, the course of thermal decomposition was qualitatively presumed. |
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抄録 | ||||||
内容記述タイプ | Abstract | |||||
内容記述 | 著者らの研究室にて,従来よりトリアジン系化合物の分解と生成についての研究を行なっている。そのうちの含イオウシァナミド誘導体(チオ尿素,チオシアン酸アンモエウム,2.4-ジチオビウレット,グアニルチオ尿素)の熱分解の研究については熱分解生成物のX線回折の測定結果が末報告であるのでここに吸収スペクトル(IR, UV)とともに総括して報告する。3種の測定手段を組み合わせる手法はこの反応については新規であってこれにより,定性的に熱分解機構を解明することができた。 | |||||
引用 | ||||||
内容記述タイプ | Other | |||||
内容記述 | 富山大学工学部紀要,22 | |||||
書誌情報 |
富山大学工学部紀要 巻 22, p. 27-32, 発行日 1971-03 |
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ISSN | ||||||
収録物識別子タイプ | ISSN | |||||
収録物識別子 | 03871339 | |||||
書誌レコードID | ||||||
収録物識別子タイプ | NCID | |||||
収録物識別子 | AN00175872 | |||||
著者版フラグ | ||||||
出版タイプ | VoR | |||||
出版タイプResource | http://purl.org/coar/version/c_970fb48d4fbd8a85 | |||||
国立国会図書館分類 | ||||||
主題Scheme | NDLC | |||||
主題 | ZM2 | |||||
出版者 | ||||||
出版者 | 富山大学工学部 | |||||
資源タイプ(DSpace) | ||||||
内容記述タイプ | Other | |||||
内容記述 | Article |